Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydroquinone → N-(3-(Dimethylamino)-2,2-dimethylpropyl)methacrylamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydroquinone | HCID 785 | — |
| 반응물 | Phosphoric Acid | HCID 1004 | — |
| 반응물 | Butyl Methacrylate | HCID 7354 | — |
| 반응물 | N,N,2,2-Tetramethylpropane-1,3-diamine | HCID 104477 | — |
| 생성물 | N-(3-(Dimethylamino)-2,2-dimethylpropyl)methacrylamide | HCID 3018570 | 60% |
반응 단계
426 g (3 mols) of butyl methacrylate, 390 g (3 mols) of N,N,2,2-tetramethylpropane-1,3-diamine, 29.4 g (0.3 mol) of H3PO4, and 2 g of hydroquinone were warmed for 2 hours at 220° C. N-(3-dimethylamino-2,2-dimethylpropyl)-methacrylic acid amide was formed in this way. Yield: 60% (selectivity: 94% calculated on the reacted butyl methacrylate).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04228102 |
| 출처 데이터셋 | uspto-grants-1980_10 |
| ORD ID | ord-88a3cdd9cbf546a985bb2883e5f2b385 |
| 출처 메모 | uspto-grants-1980_10 |