Urea → Tetrakis(ureidomethyl)phosphonium chloride

HRID 903537노트

반응식

HRID 903537 반응식
[CH2:1]([P+:3]([CH2:8]O)([CH2:6]O)[CH2:4]O)O.[Cl-:10].[NH2:11][C:12]([NH2:14])=[O:13]>C1(C)C=CC=CC=1>[Cl-:10].[NH:11]([CH2:8][P+:3]([CH2:1][NH:11][C:12]([NH2:14])=[O:13])([CH2:4][NH:11][C:12]([NH2:14])=[O:13])[CH2:6][NH:11][C:12]([NH2:14])=[O:13])[C:12]([NH2:14])=[O:13]

참가 물질

4

반응물 2

HCID 1176UreaHCID 31298Tetrakis(hydroxymethyl)phosphonium chloride

생성물 1

HCID 23463266Tetrakis(ureidomethyl)phosphonium chloride수율 101.1%

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

Reaction of THPC (9.53 g, 0.05 mol) with urea (12.01 g, 0.2 mol) in toluene (75 ml), following Example 1, gave 18.14 g (101%) of tetrakis(ureidomethyl)phosphonium chloride (I, R=R'=R"=H, X=Cl) as a colorless, brittle glass.

출처 및 근거

ORD 기록
ord-38b60aabc78f4671ad91c54b2d8d3afb
출처 데이터셋
uspto-grants-1980_10
특허 번호
US04228100

반응 노트

불러오는 중…