Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → 122570-36-9
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Dopamine Hydrochloride | HCID 65340 | — |
| 반응물 | N-acetyl-L-methionine | HCID 448580 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 122570-36-9 | HCID 22812625 | — |
반응 단계
2.85 g of dopamine hydrochloride, 4.32 g of N-hydroxysuccinimide ester of N-acetyl-L-methionine, 3.04 g of triethylamine and 15 ml of dimethylformamide are treated in the same manner as described in Example 5. After the reaction, the mixture is condensed under reduced pressure to remove solvent. The residue is dissolve in ethyl acetate, washed with water and dried. The solution is condensed to remove solvent. 3.1 g of N-(N-acetyl-L-methionyl)-dopamine are obtained as caramel.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04228183 |
| 출처 데이터셋 | uspto-grants-1980_10 |
| ORD ID | ord-6823c088a7c342818f6492ad5f3a1b94 |
| 출처 메모 | uspto-grants-1980_10 |