Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyltryptamine → 1,2,3,4-Tetrahydro-1-[3,3-bis(ethoxycarbonyl)-propyl]-2-methyl-beta-carboline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyltryptamine | HCID 6088 | — |
| 반응물 | Diethyl (3-oxopropyl)malonate | HCID 88096 | — |
| 생성물 | 1,2,3,4-Tetrahydro-1-[3,3-bis(ethoxycarbonyl)-propyl]-2-methyl-beta-carboline | HCID 23336481 | 55.2% |
반응 단계
1.78 g of N-methyl-tryptamine (i.e., 3-(2-methylaminoethyl)-indole) and 3.1 g of 4,4-bis(ethoxycarbonyl)-butanal were treated in the same manner as described in Example 21-(1). 2.1 g of 1,2,3,4-tetrahydro-1-[3,3-bis-(ethoxycarbonyl)propyl]-2-methyl-β-carboline were thereby obtained. Yield: 55.0%
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04228168 |
| 출처 데이터셋 | uspto-grants-1980_10 |
| ORD ID | ord-50ab92d2f9754825bd25d8207a0fbca9 |
| 출처 메모 | uspto-grants-1980_10 |