Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → (2-Nitrophenyl)methanesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | (2-nitrophenyl)methanesulfonyl Chloride | HCID 4305447 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | (2-Nitrophenyl)methanesulfonamide | HCID 13266249 | — |
반응 단계
To a suspension of 29.4 g of the product of Example 2 in 250 ml of diethyl ether was added 6.5 ml of anhydrous ammonia at 5°-15°. After stirring at 15°-25° for 1 hour, the product was filtered off, washed with ether, and water and oven dried at 60° to give 20.5 g of 2-nitrophenylmethanesulfonamide, m.p.=134°-136°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04420325 |
| 출처 데이터셋 | uspto-grants-1983_12 |
| ORD ID | ord-0962ea6a32954304a1470f3d92c29e71 |
| 출처 메모 | uspto-grants-1983_12 |