Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Butanol → Dibutyl Oxalate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Butanol | HCID 263 | — |
| 반응물 | Butyl nitrite | HCID 10996 | — |
| 반응물 | Butyl Formate | HCID 11614 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 반응물 | HCID 178418416 | HCID 178418416 | — |
| 생성물 | Dibutyl Oxalate | HCID 16306 | — |
반응 단계
Experiment was run in the same manner as in Example 2 except that the composition of the gaseous starting materials was replaced by 27.9% by volume of carbon monoxide, 6.2% by volume of hydrogen, 1.7% by volume of n-butyl nitrite and 64.2% by volume of nitrogen. As the result, it was found that n-butyl formate was produced in a space time yield of 109 g./l.-catalyst.hr, and small amounts of di-n-butyl oxalate and n-butanol were by-produced.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04420633 |
| 출처 데이터셋 | uspto-grants-1983_12 |
| ORD ID | ord-72d869152209498d9e4947f4fb46d16c |
| 출처 메모 | uspto-grants-1983_12 |