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Ethylmorpholine → HCID 131713280, 화합물

HRID 904959
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HRID 904959 반응식
C(N1CCOCC1)C.C1CCC(N=C=NC2CCCCC2)CC1.[NH2:24][C@H:25]([C:38]([O:40][CH3:41])=[O:39])[CH2:26][C:27]1[CH:32]=[CH:31][C:30]([O:33][C:34]([CH3:37])([CH3:36])[CH3:35])=[CH:29][CH:28]=1.Cl.[NH:43]([C:51]([O:53][CH2:54][C:55]1[CH:60]=[CH:59][CH:58]=[CH:57][CH:56]=1)=[O:52])[C@H:44]([C:48](O)=[O:49])[CH:45]([CH3:47])[CH3:46].ON1C2C=CC=CC=2N=N1>CN(C)C=O>[NH:43]([C:51]([O:53][CH2:54][C:55]1[CH:60]=[CH:59][CH:58]=[CH:57][CH:56]=1)=[O:52])[C@H:44]([C:48]([NH:24][C@H:25]([C:38]([O:40][CH3:41])=[O:39])[CH2:26][C:27]1[CH:28]=[CH:29][C:30]([O:33][C:34]([CH3:37])([CH3:35])[CH3:36])=[CH:31][CH:32]=1)=[O:49])[CH:45]([CH3:47])[CH3:46]
참가 물질반응 조건실험 절차후처리출처 및 근거반응 노트

참가 물질

7

반응물 5

HCID 7525EthylmorpholineHCID 10868DicyclohexylcarbodiimideHCID 757711-HydroxybenzotriazoleHCID 726987N-Carbobenzoxy-L-valineHCID 6452451Methyl O-tert-butyl-L-tyrosinate hydrochloride

생성물 1

HCID 131713280HCID 131713280, 화합물

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

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온도
0 °C

실험 절차

19.5 ml (approx. 150 mmoles) of N-ethylmorpholine and 33 g (160 mmoles) of DCC are added at 0° C. to a solution in 250 ml of dimethylformamide of 43.15 g (150 mmoles) of H-Tyr(But)-OMe.HCl, 37.65 g (150 mmoles) of Z-Val-OH and 20.25 g (150 mmoles) of 1-hydroxybenzotriazole. The mixture is stirred for 1 hour at 0° C. and is allowed to stand overnight at room temperature. The precipitate which has deposited is filtered off. It is rinsed with a little dimethylformamide. The filtrate is introduced into a mixture of 150 ml of saturated NaHCO3 solution and 3,000 ml of water, while stirring. The mixture is cooled to 4° C. and the precipitate is filtered off. It is washed thoroughly with water. While still wet, the product is dissolved in 400 ml of ethyl acetate. Insoluble matter is filtered off and water is separated off in a separating funnel. The ethyl acetate phase is dried over Na2SO4 and concentrated. The residue is triturated with petroleum ether and the product is filtered off. Yield 67 g (92%). Melting point 111°-112°, [α]D21 =-15.9° (c=1, methanol).

후처리

  1. waitto stand overnight at room temperature
  2. filtrationThe precipitate which has deposited is filtered off
  3. washIt is rinsed with a little dimethylformamide
  4. additionThe filtrate is introduced into a mixture of 150 ml of saturated NaHCO3 solution and 3,000 ml of water
  5. stirringwhile stirring
  6. temperatureThe mixture is cooled to 4° C.
  7. filtrationthe precipitate is filtered off
  8. washIt is washed thoroughly with water
  9. dissolutionWhile still wet, the product is dissolved in 400 ml of ethyl acetate
  10. filtrationInsoluble matter is filtered off
  11. customwater is separated off in a separating funnel
  12. dry with materialThe ethyl acetate phase is dried over Na2SO4
  13. concentrationconcentrated
  14. customThe residue is triturated with petroleum ether
  15. filtrationthe product is filtered off
  16. customMelting point 111°-112°, [α]D21 =-15.9° (c=1, methanol)

출처 및 근거

ORD 기록
ord-6b5403b036bc4e2e92e7e0d7941fe6f2
출처 데이터셋
uspto-grants-1983_12
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04420424

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