Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetone → 2,4-Di-tert-amylphenylallylether
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetone | HCID 180 | — |
| 반응물 | Allyl bromide | HCID 7841 | — |
| 반응물 | 2,4-Di-tert-pentylphenol | HCID 8455 | — |
| 반응물 | Carbonate Ion | HCID 19660 | — |
| 생성물 | 2,4-Di-tert-amylphenylallylether | HCID 70525545 | — |
반응 단계
117.2 g of 2,4-di-t-amylphenol and 90.7 g of allylbromide was dissolved in 500 ml of acetone. Thereto was added 103.5 g of pottassium carbonate and refluxed in a water bath for 20 hours. Then reaction mixture was filtered under suction and filtration residue was rinsed with 100 ml of acetone, thereafter this was again mixed with the mother solution and then under reduced pressure acetone and excess allyl bromide was distilled out.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04421846 |
| 출처 데이터셋 | uspto-grants-1983_12 |
| ORD ID | ord-6ce65696a38043df969eb3d936abe02e |
| 출처 메모 | uspto-grants-1983_12 |