4-Toluenesulfonyl chloride → 2-n-Butyl-5-tosyloxymethyl-4,5,6,7-tetrahydrobenzo[d]thiazole

HRID 905198노트

반응식

HRID 905198 반응식
[C:1]1([CH3:11])[CH:6]=[CH:5][C:4]([S:7](Cl)(=[O:9])=[O:8])=[CH:3][CH:2]=1.[CH2:12]([C:16]1[S:17][C:18]2[CH2:24][CH2:23][CH:22]([CH2:25][OH:26])[CH2:21][C:19]=2[N:20]=1)[CH2:13][CH2:14][CH3:15]>>[CH2:12]([C:16]1[S:17][C:18]2[CH2:24][CH2:23][CH:22]([CH2:25][O:26][S:7]([C:4]3[CH:5]=[CH:6][C:1]([CH3:11])=[CH:2][CH:3]=3)(=[O:9])=[O:8])[CH2:21][C:19]=2[N:20]=1)[CH2:13][CH2:14][CH3:15]

참가 물질

3

반응물 2

HCID 73974-Toluenesulfonyl chlorideHCID 129177552-n-Butyl-5-hydroxymethyl-4,5,6,7-tetrahydrobenzo[d]thiazole

생성물 1

HCID 543084972-n-Butyl-5-tosyloxymethyl-4,5,6,7-tetrahydrobenzo[d]thiazole

실험 절차

The compound is prepared by action of p-toluenesulfonyl chloride on the above derivative (IV), according to the procedure described in Example 1. It is obtained as an undistillable oil which is used crude for the subsequent reactions.

후처리

  1. customIt is obtained as an undistillable oil which

출처 및 근거

ORD 기록
ord-d4f067a8decc45afb190da028588d83f
출처 데이터셋
uspto-grants-1983_12
특허 번호
US04423056

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