N-Methyltriimidodicarbonic acid → HCID 20476324, 화합물

HRID 905349노트

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HRID 905349 반응식
[CH2:1]([NH:5][C:6]([NH:8][C:9]([NH2:11])=[O:10])=[O:7])[CH2:2][CH2:3][CH3:4].[CH3:12]NC(NC(N)=O)=O>>[CH2:1]([N:5]1[CH:12]=[N:11][C:9](=[O:10])[NH:8][C:6]1=[O:7])[CH2:2][CH2:3][CH3:4]

참가 물질

3

반응물 2

HCID 231880N-Methyltriimidodicarbonic acidHCID 4360848Imidodicarbonic diamide, N-butyl-

생성물 1

HCID 20476324HCID 20476324, 화합물수율 92%

실험 절차

Following the procedure described in Preparation 2, Part B, above, but substituting the n-butylbiuret prepared in Part A, above, for the methylbiuret, there is prepared 60 gm. (92% yield) of 1-n-butyl-5-azauracil.

후처리

  1. customdescribed in Preparation 2, Part B
  2. customprepared in Part A

출처 및 근거

ORD 기록
ord-38ad8113366f42d8826e0554cb2386c1
출처 데이터셋
uspto-grants-1983_12
특허 번호
US04423212

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