Trifluoroacetic acid → HCID 178508837, 화합물

HRID 905504

반응식

HRID 905504 반응식
[NH2:1][C:2]1[N:6]=[C:5]([NH2:7])[NH:4][N:3]=1.[F:8][C:9]([F:14])([F:13])[C:10]([OH:12])=[O:11]>O>[O-:12][C:10]([C:9]([F:14])([F:13])[F:8])=[O:11].[NH2:1][C:2]1[NH:3][NH+:4]=[C:5]([NH2:7])[N:6]=1

참가 물질

4

반응물 2

HCID 6422Trifluoroacetic acidHCID 150783,5-Diamino-1,2,4-triazole

생성물 1

HCID 178508837HCID 178508837, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

3,5-Diamino-1,2,4-triazole (1.50 g, 15.14 mmol) was dissolved in 5 ml of distilled water. Trifluoroacetic acid (1.12 ml, 15.14 mmol) was added via syringe at room temperature and the reaction was stirred at room temperature for 1 hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours.

후처리

  1. customThe water was removed in vacuo
  2. temperaturewith heating to approximately 90° C. for 4 hours

출처 및 근거

ORD 기록
ord-e08f5efc7a6e4caaaed595895ce16a64
출처 데이터셋
uspto-grants-2011_09
특허 번호
US08012277B2

연결된 노트

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