Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonium Hydroxide → 2,2-Diethoxyacetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonium Hydroxide | HCID 14923 | — |
| 반응물 | Ethyl diethoxyacetate | HCID 80169 | — |
| 생성물 | 2,2-Diethoxyacetamide | HCID 100765 | 99% |
반응 단계
Ethyl diethoxyacetate (Aldrich) (10 mL, 56.41 mmol) was added to concentrated NH4OH (50 mL) and the mixture allowed to stir until a homogeneous solution was obtained (40 hours). The solvent was then removed under reduced pressure to yield the sub-title compound as fine white needles (8.209 g, 99%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08012967B2 |
| 출처 데이터셋 | uspto-grants-2011_09 |
| ORD ID | ord-3c948a6daead4d7a9f915b6f7b70559c |
| 출처 메모 | uspto-grants-2011_09 |