Octylamine → HCID 86637176, 화합물

HRID 909117

반응식

[C:1]([O:4]CCCOC)(=[O:3])C.[OH:10][CH2:11][CH:12]1[CH2:16][O:15]C(=O)[O:13]1.[CH2:18]([NH2:26])[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25]>>[OH:10][CH2:11][CH:12]([CH2:16][OH:15])[OH:13].[CH2:18]([NH:26][C:1](=[O:3])[O-:4])[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25]

참가 물질

반응물 3

HCID 8143Octylamine

HCID 97944Glycerol carbonate

HCID 536841Npc129341

생성물 1

HCID 86637176HCID 86637176, 화합물

반응 조건

온도: 70 °C

실험 절차

354 g of methoxypropyl acetate, 237 g (2 moles) of glycerol carbonate (Jeffsol GC from Huntsman; CAS RN: 931-40-8; molecular weight: 118.09) are introduced in succession, under nitrogen, into a three-necked flask equipped with a condenser and an addition funnel. The mixture is stirred at 230 revolutions per minute and heated to 70° C. Then 262.5 g (2.03 moles) of n-octylamine (CAS RN: 11-86-4; molecular weight: 129.25) are added to the reaction mixture in the course of 15 minutes. The reaction is strongly exothermic and the temperature of the reaction mixture reaches approximately 88° C.

후처리

customequipped with a condenser and an addition funnel
customreaches approximately 88° C.

출처 및 근거

ORD 기록: ord-bdfbb304a8a44981b4503b9ab65f5667
출처 데이터셋: uspto-grants-2011_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08017719B2

연결된 노트

불러오는 중…