Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(Chloromethyl)phenyl acetate → HCID 57656056, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(Chloromethyl)phenyl acetate | HCID 148312 | — |
| 반응물 | 3-tert-butoxycarbonyl-7-chloro-6-dimethylaminocarbonylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine | HCID 57655979 | — |
| 생성물 | HCID 57656056 | HCID 57656056 | — |
반응 단계
Use a method similar to the Preparation 177, using 3-tert-butoxycarbonyl-7-chloro-6-dimethylcarbamoylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine and 4-(chloromethyl)phenyl acetate to give 6-(4-acetoxybenzylthio)-3-tert-butoxycarbonyl-7-chloro-2,3,4,5-tetrahydro-1H-benzo[d]azepine as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08022062B2 |
| 출처 데이터셋 | uspto-grants-2011_09 |
| ORD ID | ord-897100b63ff64991a19ac421ecb45a9b |
| 출처 메모 | uspto-grants-2011_09 |