Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → N-(3,5-dimethoxyphenyl)acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | Hexane | HCID 8058 | — |
| 반응물 | 3,5-Dimethoxyaniline | HCID 66301 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N-(3,5-dimethoxyphenyl)acetamide | HCID 702039 | — |
반응 단계
To a solution of 3,5-dimethoxy-phenylamine (22.0 g, 143.6 mmol) in toluene (100 mL), is added slowly Ac2O (14 mL) at room temperature. After stirring 30 minutes, hexane (50 mL) is added with stirring at room temperature. The resulting solid is filtered and washed with hexane (50 mL) to offer designed product as a white solid 14.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08026243B2 |
| 출처 데이터셋 | uspto-grants-2011_09 |
| ORD ID | ord-64bcb4283a7945a9bd9298d6aa0737d0 |
| 출처 메모 | uspto-grants-2011_09 |