Ammonia → HCID 178514164, 화합물
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[N:1]1[NH:2][C:3](NC)=[CH:4][CH:5]=1.[C:8]([N:16]=[C:17]=[S:18])(=O)C1C=CC=CC=1.[NH3:19]>CO>[NH:1]1[CH:5]=[CH:4][C:3]([CH2:8][NH:16][C:17]([NH2:19])=[S:18])=[N:2]1참가 물질
5
실험 절차
The title compound was prepared in accordance with the general method described in Example 12(a) by using 2H-pyrazol-3-yl-methylamine (1.20 g, 12.4 mmol), benzoyl isothiocyanate (1.8 mL, 13.6 mmol) and ammonia in methanol (7N, 60 mL) with the exception that the crude product isolated by filtration (1.39 g, 72% yield) was used in the next step without further purification. MS (ESI) m/z 157 (M+1)
후처리
- customisolated by filtration (1.39 g, 72% yield)
- customwas used in the next step without further purification
출처 및 근거
- ORD 기록
- ord-4e26e5919d2b42cf8a9cf0d7caae231b
- 출처 데이터셋
- uspto-grants-2011_09
- 특허 번호
- US08026244B2
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