Hydrazine → HCID 27055575, 화합물
반응식
[CH2:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4][CH2:3][N:2]1[CH2:11][C:12]([O:14]CC)=O.[NH2:17][NH2:18]>C(O)C>[CH2:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4][CH2:3][N:2]1[CH2:11][C:12]([NH:17][NH2:18])=[O:14]참가 물질
4
실험 절차
A solution of 90 (2.0 g, 9.12 mmol) and hydrazine (5.1 g, 91 mmol) in ethanol (30 mL) was heated at reflux overnight. The mixture was concentrated under reduced pressure to give 91 (1.87 g ˜100%) which was used without further purification.
후처리
- temperatureat reflux overnight
- concentrationThe mixture was concentrated under reduced pressure
출처 및 근거
- ORD 기록
- ord-62c165ed74a74b769d7b88b2dc611239
- 출처 데이터셋
- uspto-grants-2007_09
- 특허 번호
- US07265122B2
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