Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tetrahydrofuran → Citraconic Acid Hydroxyethyl Methacrylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tetrahydrofuran | HCID 8028 | — |
| 반응물 | 2-Hydroxyethyl Methacrylate | HCID 13360 | — |
| 반응물 | Citraconic acid | HCID 643798 | — |
| 촉매 | Azobisisobutyronitrile | HCID 6547 | — |
| 용매 | Diethylethylether | HCID 12430074 | — |
| 생성물 | Citraconic Acid Hydroxyethyl Methacrylate | HCID 86602179 | 96% |
반응 단계
To 20 g of tetrahydrofuran (THF) were added 5 g of citraconic acid, 5 g of hydroxyethyl methacrylate and 0.1 g of AIBN. The resulting mixture was reacted at 67° C. for 3 hours, after which, the resulting solution was dropped in diethylethyl ether, thereby obtaining 9.6 g of a photoresist polymer of Formula (IIc).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07270934B2 |
| 출처 데이터셋 | uspto-grants-2007_09 |
| ORD ID | ord-bee63e5f9a174a5e828a7e7b25d3b5a0 |
| 출처 메모 | uspto-grants-2007_09 |