3-Butyn-2-amine, 2-methyl- → HCID 86607368, 화합물

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[Cl:1][C:2]1[CH:3]=[C:4]([CH:19]=[C:20]([Cl:22])[CH:21]=1)[O:5][CH:6]([CH2:16][O:17][CH3:18])[C:7]([NH:9][C:10]([CH3:15])([CH3:14])[C:11]#[C:12]C)=[O:8].NC(C)(C)C#C.NC(C)(C)C#CC>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:19]=[C:20]([Cl:22])[CH:21]=1)[O:5][CH:6]([CH2:16][O:17][CH3:18])[C:7]([NH:9][C:10]([CH3:14])([CH3:15])[C:11]#[CH:12])=[O:8]

참가 물질

반응물 3

HCID 763193-Butyn-2-amine, 2-methyl-

HCID 114123462-Methylpent-3-yn-2-amine

HCID 69114589HCID 69114589, 화합물

생성물 1

HCID 86607368HCID 86607368, 화합물

실험 절차

2-(3,5-Dichlorophenoxy)-3-methoxy-N-(3-methylbut-1-yn-3-yl)propionamide was prepared in a similar way to 2-(3,5-dichlorophenoxy)-3-methoxy-N-(4-methylpent-2-yn-4-yl)propionamide as described in Example 1 except that 3-amino-3-methylbut-1-yne (commercially available as 90% aqueous solution) was used in place of 4-amino-4-methyl pent-2-yne in Stage 4.

출처 및 근거

ORD 기록: ord-3f555933faad48b087c2aa249a019f4c
출처 데이터셋: uspto-grants-2007_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07271130B2

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