Allyl bromide → 2-(Nitromethylidene)-1-(prop-2-en-1-yl)-1,3-diazepane

HRID 918363노트

반응식

HRID 918363 반응식
[N+:1]([CH:4]=[C:5]1[NH:11][CH2:10][CH2:9][CH2:8][CH2:7][NH:6]1)([O-:3])=[O:2].[CH2:12](Br)[CH:13]=[CH2:14]>>[N+:1]([CH:4]=[C:5]1[NH:6][CH2:7][CH2:8][CH2:9][CH2:10][N:11]1[CH2:14][CH:13]=[CH2:12])([O-:3])=[O:2]

참가 물질

3

반응물 2

HCID 7841Allyl bromideHCID 116583251H-1,3-Diazepine, hexahydro-2-(nitromethylene)-

생성물 1

HCID 706385112-(Nitromethylidene)-1-(prop-2-en-1-yl)-1,3-diazepane

실험 절차

Method B, reacting hexahydro-2-(nitromethylene)-1H-1,3-diazepine with allyl bromide. Melting point: 82°-83°.

출처 및 근거

ORD 기록
ord-f67aa86a27854bb6835d89341366431e
출처 데이터셋
uspto-grants-1976_07
특허 번호
US03971774

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