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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 919385생성일: 2026년 10월 26일

5-Nitrofuroyl chloride → N'2-(6-trifluoromethoxy-1,3-benzothiazol-2yl)-5-nitro-2-furanecarbohydrazide

https://huagongshe.com/reaction/919385

반응식

참여 물질

역할이름HCID투입량
반응물5-Nitrofuroyl chlorideHCID 90711—
반응물2-Hydrazinyl-6-(trifluoromethoxy)-1,3-benzothiazoleHCID 10422158—
생성물N'2-(6-trifluoromethoxy-1,3-benzothiazol-2yl)-5-nitro-2-furanecarbohydrazideHCID 86664241—

반응 조건

온도0 °C

반응 단계

The compound 4e was prepared according to above described method by using 5-nitro-2-furancarboxylic acid chloride (430 mg, 1 mmol) and 2-hydrazino-6-trifluoromethoxybenzothiazole (319 mg, 1.5 mmol) which stirred for 1 h at 0° C. and stirring continued at 25° C. for 11 h (yield 287 mg, 87%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US09273039B2
출처 데이터셋uspto-grants-2016_03
ORD IDord-81e5f642467645afbd721bce4d22419d
출처 메모uspto-grants-2016_03