홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Ammonium Chloride → Benzyl [(3S)-1-(3-amino-5-cyanopyridin-4-yl)piperidin-3-yl]carbamate

HRID 924439
노트
인쇄 미리보기

반응식

HRID 924439 반응식
[C:1]([C:3]1[CH:4]=[N:5][CH:6]=[C:7]([N+:26]([O-])=O)[C:8]=1[N:9]1[CH2:14][CH2:13][CH2:12][C@H:11]([NH:15][C:16](=[O:25])[O:17][CH2:18][C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[CH2:10]1)#[N:2].[Cl-].[NH4+]>CCO.O.[Fe]>[NH2:26][C:7]1[CH:6]=[N:5][CH:4]=[C:3]([C:1]#[N:2])[C:8]=1[N:9]1[CH2:14][CH2:13][CH2:12][C@H:11]([NH:15][C:16](=[O:25])[O:17][CH2:18][C:19]2[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=2)[CH2:10]1
참가 물질반응 조건실험 절차후처리출처 및 근거반응 노트

참가 물질

6

반응물 2

HCID 25517Ammonium ChlorideHCID 86726889Benzyl [(3S)-1-(3-cyano-5-nitropyridin-4-yl)piperidin-3-yl]carbamate

생성물 1

HCID 86726890Benzyl [(3S)-1-(3-amino-5-cyanopyridin-4-yl)piperidin-3-yl]carbamate수율 92.1%

시약·촉매·용매 3

HCID 23925Iron촉매HCID 702Ethanol용매
HCID 962
Water
용매

반응 조건

온도
85 °C

실험 절차

A mixture of benzyl [(3S)-1-(3-cyano-5-nitropyridin-4-yl)piperidin-3-yl]carbamate (0.065 g, 0.17 mmol), iron (0.084 g, 1.5 mmol), and ammonium chloride (0.091 g, 1.7 mmol) in EtOH (2 mL) and water (0.2 mL) was stirred at 85° C. for 15 min. The crude reaction mixture was filtered through a pad of diatomaceous earth and the inorganics were washed thoroughly with EtOH. The filtrate was concentrated under reduced pressure and the residue was partitioned between water and EtOAc. The organic fraction was washed with water, brine, dried over Na2SO4, filtered, and concentrated under reduced pressure to afford the sub-title compound (0.055 g). LCMS (ESI) calc. for C19H22N5O2 m/z=352.2 [M+H]+. found 352.1.

후처리

  1. customThe crude reaction mixture
  2. filtrationwas filtered through a pad of diatomaceous earth
  3. washthe inorganics were washed thoroughly with EtOH
  4. concentrationThe filtrate was concentrated under reduced pressure
  5. customthe residue was partitioned between water and EtOAc
  6. washThe organic fraction was washed with water, brine
  7. dry with materialdried over Na2SO4
  8. filtrationfiltered
  9. concentrationconcentrated under reduced pressure

출처 및 근거

ORD 기록
ord-3dfba6df65cb4832a51ef3b8c1594ce4
출처 데이터셋
uspto-grants-2016_03
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US09278950B2

반응 노트

불러오는 중…

이 페이지에서참가 물질반응 조건실험 절차후처리출처 및 근거반응 노트