Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,2-Dichlorobenzene → 2,4-Dihydroxy-3-allylbenzophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,2-Dichlorobenzene | HCID 7239 | — |
| 반응물 | 4-Allyloxy-2-hydroxybenzophenone | HCID 75689 | — |
| 생성물 | 2,4-Dihydroxy-3-allylbenzophenone | HCID 21910981 | — |
반응 단계
Commercially available 4-allyloxy-2-hydroxybenzophenone (15 g) was rearranged by heating under reflux in ortho-dichlorobenzene (60 mL) for 26 hours. The product was isolated by dilution of the reaction mixture with 5 volumes hexanes to give a crystalline product as fine needles.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07091230B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-83d069dc05c04271afbe84952104b3b2 |
| 출처 메모 | uspto-grants-2006_08 |