Ethyl Acetate → HCID 86669356, 화합물

반응식

[OH:1][C:2]1[C:9]([O:10][CH2:11][CH2:12]C)=[CH:8][C:5]([CH:6]=[O:7])=[CH:4][C:3]=1[N+]([O-])=O.C[CH2:18][O:19]C(C)=O>>[OH:1][C:2]1[CH:3]=[CH:4][C:5]([CH:6]=[O:7])=[CH:8][C:9]=1[O:10][CH2:11][CH2:12][O:19][CH3:18]

참가 물질

반응물 2

HCID 8857Ethyl Acetate

HCID 573549704-Hydroxy-3-nitro-5-propoxybenzaldehyde

생성물 1

HCID 86669356HCID 86669356, 화합물수율 97%

실험 절차

Followed the procedure described in Step 3 of Intermediate 65, where the reaction was refluxed for 2 days. Isolated 900 mg, yield 97% after column chromatography (PE:EtOAc=10:1).

후처리

temperaturewas refluxed for 2 days

출처 및 근거

ORD 기록: ord-eb28c95408d344f19918fa614793ab88
출처 데이터셋: uspto-grants-2016_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09283229B2

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