Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Propionic Acid → 3-Fluoro-2,6-dipropyl-4-propionylphenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Propionic Acid | HCID 1032 | — |
| 반응물 | Trifluoromethanesulfonic acid | HCID 62406 | — |
| 반응물 | 3-Fluoro-2,4-dipropylphenol | HCID 21985957 | — |
| 생성물 | 3-Fluoro-2,6-dipropyl-4-propionylphenol | HCID 21985943 | — |
반응 단계
Propionic acid (9.07 g, 123 mmol) and 3-fluoro-2,4-dipropylphenol (9.60 g, 49.0 mmol) were mixed in trifluoromethanesulfonic acid (50 mL) as in Example 13, step 1. Purification by chramotography on silica gel using ethyl acetate:hexane (10:90) gave the title compound as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07091230B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-f951ff6e45a44e29983784a13e42f834 |
| 출처 메모 | uspto-grants-2006_08 |