Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Iodo-1,2-dimethoxybenzene → 3,4-bis(Benzyloxy)-6-[2-(3,4-dimethoxyphenyl)ethynyl]pyridazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Iodo-1,2-dimethoxybenzene | HCID 230307 | — |
| 반응물 | 3,4-Bis(benzyloxy)-6-{[5-(trifluoromethyl)pyridin-2-yl]ethynyl}pyridazine | HCID 71269910 | — |
| 반응물 | 3,4-Bis(benzyloxy)-6-ethynylpyridazine | HCID 86677025 | — |
| 생성물 | 3,4-bis(Benzyloxy)-6-[2-(3,4-dimethoxyphenyl)ethynyl]pyridazine | HCID 71270121 | 17% |
반응 단계
Prepared as described for 3,4-bis(benzyloxy)-6-{[5-(trifluoromethyl)pyridin-2-yl]ethynyl}pyridazine (Intermediate 6) from 3,4-bis(benzyloxy)-6-ethynylpyridazine (Intermediate 5) and 4-iodo-1,2-dimethoxybenzene in 17% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09290456B2 |
| 출처 데이터셋 | uspto-grants-2016_03 |
| ORD ID | ord-10bb13aa6f14400a9d4fed4e9ef9142b |
| 출처 메모 | uspto-grants-2016_03 |