Methyl 6-[bis-(tert-butoxycarbonyl)amino]-2-hydroxy-3-(2-hydroxymethylfuran-3-yl)benzoate → Methyl 2-[bis-(tert-butyoxycarbonyl)amino]-6-hydroxybenzoate

HRID 927942노트

반응식

HRID 927942 반응식
[C:1]([O:5][C:6]([N:8]([C:27]([O:29][C:30]([CH3:33])([CH3:32])[CH3:31])=[O:28])[C:9]1[C:14]([C:15]([O:17][CH3:18])=[O:16])=[C:13]([OH:19])[C:12](C2C=COC=2CO)=[CH:11][CH:10]=1)=[O:7])([CH3:4])([CH3:3])[CH3:2].C(OC(N(C(OC(C)(C)C)=O)C1C=CC=C(OS(C2C=CC(C)=CC=2)(=O)=O)C=1C(OC)=O)=O)(C)(C)C>>[C:1]([O:5][C:6]([N:8]([C:27]([O:29][C:30]([CH3:33])([CH3:32])[CH3:31])=[O:28])[C:9]1[CH:10]=[CH:11][CH:12]=[C:13]([OH:19])[C:14]=1[C:15]([O:17][CH3:18])=[O:16])=[O:7])([CH3:3])([CH3:4])[CH3:2]

참가 물질

3

반응물 2

HCID 66685556Methyl 6-[bis-(tert-butoxycarbonyl)amino]-2-hydroxy-3-(2-hydroxymethylfuran-3-yl)benzoateHCID 86713299Methyl 2-[bis-(tert-butoxycarbonyl)amino]-6-(4-methylbenzenesulfonyloxy)-benzoate2회

생성물 1

HCID 71006903Methyl 2-[bis-(tert-butyoxycarbonyl)amino]-6-hydroxybenzoate

실험 절차

Prepared by proceeding in a similar manner to Intermediate 4, starting from methyl 2-[bis-(tert-butoxycarbonyl)amino]-6-(4-methylbenzenesulfonyloxy)benzoate (Intermediate 56)

후처리

  1. customPrepared

출처 및 근거

ORD 기록
ord-880f9489ba05458ab5836c2f49912551
출처 데이터셋
uspto-grants-2016_03
특허 번호
US09290472B2

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