Methyl 3-chloro-5-methoxypicolinate → 3-Chloro-5-methoxypicolinic acid

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FC(F)(F)COC1C(C(N)=O)=NC=CC=1.[Cl:16][C:17]1[C:18]([C:25]([O:27]C)=[O:26])=[N:19][CH:20]=[C:21]([O:23][CH3:24])[CH:22]=1>>[Cl:16][C:17]1[C:18]([C:25]([OH:27])=[O:26])=[N:19][CH:20]=[C:21]([O:23][CH3:24])[CH:22]=1

참가 물질

반응물 2

HCID 21696614Methyl 3-chloro-5-methoxypicolinate

HCID 66644029HCID 66644029, 화합물

생성물 1

HCID 676098923-Chloro-5-methoxypicolinic acid

실험 절차

Using an analogous reaction to that described for Intermediate 5, step 2 methyl 3-chloro-5-methoxypicolinate was converted to the title compound. MS m/z=188 (M+H).

후처리

customan analogous reaction to

출처 및 근거

ORD 기록: ord-900e2a4f1bb1401e8b8cb2d1fc49d0f3
출처 데이터셋: uspto-grants-2016_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09296734B2

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