참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ethoxyacetyl chloride | HCID 84189 | — |
| 반응물 | 7-Bromo-n4-(cyclohexylmethyl)quinoline-3,4-diamine | HCID 68817887 | — |
| 생성물 | 7-bromo-1-cylcohexylmethyl-2-ethoxymethyl-1H-imidazo[4,5-c]quinoline | HCID 131725889 | — |
반응 단계
A modification of the method described in Part A of Example 9 was used to treat 7-bromo-N4-(cyclohexylmethyl)quinoline-3,4-diamine (7.3 g, 22 mmol) with ethoxyacetyl chloride (2.75 mL, 24.0 mmol). The reaction was heated overnight at 90° C. and then concentrated under reduced pressure to provide 7-bromo-1-cylcohexylmethyl-2-ethoxymethyl-1H-imidazo[4,5-c]quinoline as a dark brown semi-solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07091214B2 |
|---|
| 출처 데이터셋 | uspto-grants-2006_08 |
|---|
| ORD ID | ord-f41eaa09f57b47d7a510a6dea1c16c23 |
|---|
| 출처 메모 | uspto-grants-2006_08 |
|---|
