Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Adamantanone → N'-(adamantan-2-ylidene)(tert-butoxy)carbohydrazide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Adamantanone | HCID 64151 | — |
| 반응물 | tert-Butyl carbazate | HCID 70091 | — |
| 용매 | Hexane | HCID 8058 | — |
| 생성물 | N'-(adamantan-2-ylidene)(tert-butoxy)carbohydrazide | HCID 8039095 | — |
반응 단계
A hexane solution containing 2-adamantanone (2 g) and tert-butyl carbazate (1.76) was heated to reflux for 3 hours. When the solution cooled, the title compound crystallized and was filtered (3.28 g). M. p. 175-177°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05760059 |
| 출처 데이터셋 | uspto-grants-1998_06 |
| ORD ID | ord-704dd1d4bb5545e08cbb6cdc82f57b0e |
| 출처 메모 | uspto-grants-1998_06 |