1,2-Dichloroethane → HCID 131716892, 화합물

HRID 962885노트

반응식

HRID 962885 반응식
[CH2:1]([Cl:4])[CH2:2][Cl:3].[CH3:5][O:6][C:7](=[O:15])[C@H:8]([CH2:10][CH2:11][CH2:12][CH2:13][NH2:14])[NH2:9]>O>[CH2:1]([Cl:4])[CH2:2][Cl:3].[CH3:5][O:6][C:7](=[O:15])[C@H:8]([CH2:10][CH2:11][CH2:12][CH2:13][NH2:14])[NH2:9]

참가 물질

4

반응물 2

HCID 111,2-Dichloroethane4회HCID 117779L-Lysine, methyl ester3회

생성물 1

HCID 131716892HCID 131716892, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

A 0.4%(w/w) solution of HA in water was prepared. The pH of this solution was adjusted to between 4.3 and 4.75 by addition of acid. To each 100 ml of this solution was added 0.76 g of EDC with stirring until the EDC had completely dissolved. To each 100 ml of the HA/EDC solution was added 0.20 g of lysine methyl ester (LME) with stirring until the LME had completely dissolved. The addition of HA, EDC, and LME was conducted at room temperature; once the final HA/EDC/LME solution had been formed, it was stored at 4° C. until needed.

후처리

  1. additionThe pH of this solution was adjusted to between 4.3 and 4.75 by addition of acid
  2. dissolutionhad completely dissolved
  3. dissolutionhad completely dissolved
  4. customwas conducted at room temperature

출처 및 근거

ORD 기록
ord-44012eb552e34ba981741ecaa79c1d07
출처 데이터셋
uspto-grants-1998_06
특허 번호
US05760200

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