Chlorotrimethylsilane → (3-Iodophenyl)(trimethyl)silane

HRID 963002노트

반응식

Cl[Si:2]([CH3:5])([CH3:4])[CH3:3].[I:6][C:7]1[CH:12]=[CH:11][CH:10]=[C:9](I)[CH:8]=1>>[I:6][C:7]1[CH:12]=[CH:11][CH:10]=[C:9]([Si:2]([CH3:5])([CH3:4])[CH3:3])[CH:8]=1

참가 물질

반응물 2

HCID 6397Chlorotrimethylsilane

HCID 12270Benzene, 1,3-diiodo-

생성물 1

HCID 12358196(3-Iodophenyl)(trimethyl)silane

실험 절차

1-Iodo-3-trimethylsilanyl-benzene is prepared in a manner analogous to the procedure described in examples 1 and 1a utilizing chlorotrimethylsilane and 1,3-diiodobenzene as the dihalo compound of formula (III).

출처 및 근거

ORD 기록: ord-026811d97b754223aa6be5fba03537c5
출처 데이터셋: uspto-grants-1998_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05760267

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