Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 9637생성일: 2026년 10월 23일
1-(4-(Trifluoromethyl)phenyl)ethan-1-one → 3-Dimethylamino-1-(4-trifluoromethyl-phenyl)-but-2-en-1-one
https://huagongshe.com/ko/reaction/9637
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1-(4-(Trifluoromethyl)phenyl)ethan-1-one | HCID 69731 | — |
| 반응물 | 1,1-Dimethoxyethyl(dimethyl)amine | HCID 87835 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 3-Dimethylamino-1-(4-trifluoromethyl-phenyl)-but-2-en-1-one | HCID 69234633 | — |
반응 단계
A mixture of 4′-(trifluoromethyl)acetophenone (9.8 g) and N-(1,1-dimethoxyethyl)-N,N-dimethylamine (8.2 g) was heated at 112° C. overnight, under nitrogen. The reaction mixture was cooled and concentrated giving an orange solid. Trituration with diethyl ether gave the title compound as a yellow solid
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US07091237B2 |
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| 출처 데이터셋 | uspto-grants-2006_08 |
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| ORD ID | ord-1ea84c7acf084517a9e9625c59ac88bf |
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| 출처 메모 | uspto-grants-2006_08 |
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