Benzene → 1-(3-Acetoxy-2-fluoroprop-1-enyl)-1-(4-fluorophenyl)cyclopropane
반응식
[C:1](Cl)(=[O:3])[CH3:2].[F:5][C:6]([CH2:18][OH:19])=[CH:7][C:8]1([C:11]2[CH:16]=[CH:15][C:14]([F:17])=[CH:13][CH:12]=2)[CH2:10][CH2:9]1.C1C=CC=CC=1>N1C=CC=CC=1>[C:1]([O:19][CH2:18][C:6]([F:5])=[CH:7][C:8]1([C:11]2[CH:12]=[CH:13][C:14]([F:17])=[CH:15][CH:16]=2)[CH2:10][CH2:9]1)(=[O:3])[CH3:2]참가 물질
5
실험 절차
The method of Example 17 was repeated using acetyl chloride (0.46 ml), 1-(2-fluoro-3-hydroxyprop-1-enyl)-1-(4-fluorophenyl)cyclopropane (Example 12) (0.2 g), benzene (12 ml) and pyridine to yield the title compound (0.23 g, 96%).
출처 및 근거
- ORD 기록
- ord-f922490b341b432badd47ae777cb601b
- 출처 데이터셋
- uspto-grants-1998_06
- 특허 번호
- US05763700
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