Water → HCID 86752776, 화합물

HRID 963913

반응식

HRID 963913 반응식
C1C=C([N+]([O-])=O)N(CCO)C=1C(N)=O.O.[C:16]([CH2:19][C:20](=[O:22])[CH3:21])(=[O:18])[CH3:17].CCCCOC(C1C(C(OCC2C=CC=CC=2)=O)=CC=CC=1)=O>CC(C)=O>[C:16]([CH2:19][C:20](=[O:22])[CH3:21])(=[O:18])[CH3:17].[CH3:17][C:16]([CH3:19])=[O:18]

참가 물질

7

반응물 5

HCID 962Water2회HCID 2347Butyl Benzyl PhthalateHCID 31261AcetylacetoneHCID 1606551-(2-Hydroxyethyl)-5-nitro-1H-pyrrole-2-carboxamideHCID 178435178HCID 178435178, 화합물

생성물 1

HCID 86752776HCID 86752776, 화합물

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

On the first day, 1.31 grams of dispersant, NP-10 (Union Carbide), 1.6 grams of high-resistivity water (very pure water prepared in-house for semiconductor work) and 15 grams of solvent mixture (made from 172 ml acetone and 28 ml acetylacetone) were added and mixed well in a 250 ml polypropylene bottle. Then, 13.0 grams of borosilicate glass powder and 8.75 grams of quartz were added into the mixture and ball milled overnight using 10 mm diameter ZrO2 balls. On the second day, 0.2 gram of binder, Butvar B79 (Monsanto) was added into the mixture and ball milled for one hour. Then 2.41 grams of B79, 2.61 grams of plasticizer, Santicizer 160 (butyl phthalate from Monsanto) were added into the bottle and milled for about 3 hours to obtain a creamy, smooth mixture known as a slip or slurry. The slip was cast on a carrier of Fujimori Mylar™ using a 6 inch wide doctor blade having a 16 mil gap at 14 ft/min at room temperature.

후처리

  1. additionwere added
  2. custommilled overnight
  3. additionOn the second day, 0.2 gram of binder, Butvar B79 (Monsanto) was added into the mixture and ball
  4. custommilled for one hour
  5. custommilled for about 3 hours
  6. customto obtain a creamy, smooth mixture
  7. customat room temperature

출처 및 근거

ORD 기록
ord-fc9f3bca285e4359abfa9a73511196ee
출처 데이터셋
uspto-grants-1998_06
특허 번호
US05766528

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