Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalyl chloride → 2,2-Dimethyl-4-benzyloxycarbonylbutyryl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | 2,2-Dimethyl-4-benzyloxycarbonylbutyric acid | HCID 19080045 | — |
| 생성물 | 2,2-Dimethyl-4-benzyloxycarbonylbutyryl chloride | HCID 19080038 | — |
반응 단계
A mixture of 3.1 g of 2,2-dimethyl-4-benzyloxycarbonylbutyric acid and 3.3 ml of oxalyl chloride was refuxed for 1 h. After being cooled to room temperature, the solution was concentrated in vacuo and dried overnight The obtained oil was not further purified for the next reaction.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05767256 |
| 출처 데이터셋 | uspto-grants-1998_06 |
| ORD ID | ord-3e46a729568240518792c9616546daaf |
| 출처 메모 | uspto-grants-1998_06 |