Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl 2-acetylhexanoate → HCID 178441161, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl 2-acetylhexanoate | HCID 95466 | — |
| 반응물 | Carbonic acid-guanidine (1:1) | HCID 286947 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178441161 | HCID 178441161 | 47.6% |
반응 단계
A mixture of ethyl 2-acetylhexanoate (5.59 g, 30 mmol), guanidine carbonate (6.49 g, 30 mmol) and ethanol (20 ml) was refluxed for 11 hours and then ice-cooled. The precipitated crystals were filtered, washed with ethanol and dried in vacuo to give 2-amino-5-butyl-6-methylpyrimidine-4-ol (2.59 g, 47%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06951866B2 |
| 출처 데이터셋 | uspto-grants-2005_10 |
| ORD ID | ord-3efbba5677c24c3e998d3b7c5509d1a6 |
| 출처 메모 | uspto-grants-2005_10 |