Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methylpyridine 1-oxide → 2-[2-(4-Methoxy-phenyl)-vinyl]-pyridine 1-oxide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methylpyridine 1-oxide | HCID 13602 | — |
| 반응물 | 4-Methoxybenzaldehyde | HCID 31244 | — |
| 반응물 | Potassium tert-butoxide | HCID 23665647 | — |
| 생성물 | 2-[2-(4-Methoxy-phenyl)-vinyl]-pyridine 1-oxide | HCID 69592112 | — |
반응 단계
Following the general method described in example 2a, 2-picoline-1-oxide was reacted with potassium tert.-butanolate and p-anisaldehyde. After extraction and chromatography the title compound was obtained as a yellow solid material. MS: m/e=227 (M+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06951875B2 |
| 출처 데이터셋 | uspto-grants-2005_10 |
| ORD ID | ord-d36fc8c92df14c929ae703075c83232c |
| 출처 메모 | uspto-grants-2005_10 |