2,4,6-Tri-tert-butylphenol → HCID 178506938, 화합물

참여 물질

반응 단계

Both 10 mmol (2.2 g) of monocyclopentadienyl titanium chloride(CpTiCl3) and 100 ml of toluene were added to a 200 ml Schlenk reactor in the atmosphere of inert gas. Then, 10 mmol of 2,4,6-tri-t-butyl phenoxy lithium, so obtained from the reaction between 2,4,6-tri-t-butyl phenol and n-butyl lithium, was slowly added to the mixture. The reactional solution was stirred at room temperature and stood for 1 hour. After 1 hour, some mixture was collected and was analyzed by 1H-NMR spectroscopy to ascertain the reaction results.

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