참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Ethylphenol | HCID 6997 | — |
| 반응물 | Ethyl bromoacetate | HCID 7748 | — |
| 반응물 | Cesium carbonate | HCID 10796 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | Ethyl (2-ethylphenoxy)acetate | HCID 21986411 | — |
반응 단계
A mixture of 2-ethylphenol (244 mg) in acetonitrile (20 ml) was treated with cesium carbonate (650 mg) and ethyl bromoacetate (0.221 ml) and the mixture stirred at 60° C. for 6 hours and then at ambient temperature for 17 hours. The reaction mixture was diluted with ethyl acetate; the suspension filtered and the title compound isolated by evaporation in vacuo of the filtrate as a colourless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07091237B2 |
|---|
| 출처 데이터셋 | uspto-grants-2006_08 |
|---|
| ORD ID | ord-9cda42749fb643e8a2f6c6ec8e8fcd8b |
|---|
| 출처 메모 | uspto-grants-2006_08 |
|---|