Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Hydroxyhexanoic acid → 5-Butyloxazolidine-2,4-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Hydroxyhexanoic acid | HCID 99824 | — |
| 반응물 | Hexanamide, 2-hydroxy- | HCID 9833961 | — |
| 반응물 | 5-Butyl-oxazolidin-2,4-dione sodium salt | HCID 69745152 | — |
| 생성물 | 5-Butyloxazolidine-2,4-dione | HCID 9942204 | — |
반응 단계
A part of the reaction solution was sampled and the components of the reaction solution were analyzed by HPLC, as a result, the concentration of the starting material 2-hydroxyhexanoic acid amide was 1.6 mass % in the solution, the concentration of 5-butyl-oxazolidin-2,4-dione sodium salt as the objective product was 24.0 mass % in the solution and the concentration of 2-hydroxyhexanoic acid was 2.3 mass % in the solution. From these analysis values, the conversion of 2-hydroxyhexanoic acid amide was 92.6% and the yield in terms of 5-butyl-oxazolidin-2,4-dione was 82.1%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06953859B2 |
| 출처 데이터셋 | uspto-grants-2005_10 |
| ORD ID | ord-ff9ac95875e74c2f847a4266786d5038 |
| 출처 메모 | uspto-grants-2005_10 |