Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium 4-methylbenzenesulfonate → 4-Methylphenylbenzylpiperidinium tosylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium 4-methylbenzenesulfonate | HCID 3720192 | — |
| 반응물 | 4-Methylphenylbenzylpiperidinium bromide | HCID 86588824 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 4-Methylphenylbenzylpiperidinium tosylate | HCID 86588825 | 91,980.203% |
반응 단계
An aqueous solution prepared by dissolving 4-methylphenylbenzylpiperidinium bromide (13.85 g, 0.04 mmol) and sodium p-toluenesulfonate (9.32 g, 0.048 mmol) in 50 ml of deionized water was extracted with 50 ml of chloroform twice by using a separating funnel. The resulting chloroform phases were combined and the combined solution was washed with 50 ml of deionized water, followed by filtration and drying to obtain 4-methylphenylbenzylpiperidinium tosylate (16.1 g, yield: 92%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06958205B2 |
| 출처 데이터셋 | uspto-grants-2005_10 |
| ORD ID | ord-b93f0cc87f6a45a998414276fb93508a |
| 출처 메모 | uspto-grants-2005_10 |