Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 10910823, 화합물 → Spermine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 10910823 | HCID 10910823 | — |
| 반응물 | TriBoc-Spermine | HCID 22610912 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | Spermine | HCID 1103 | — |
반응 단계
Monoquaternary spermine containing hydrophilic head-group was prepared in a similar way to compound 3. Briefly, TriBoc-Spermine was reacted with excess of 1-azido-3-iodo-propane in the presence of excess TBA. The resulting quaternarized derivative was hydrogenised under (Pd—C) and Boc protecting group were removed using gaseous HCl in dry methanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06958325B2 |
| 출처 데이터셋 | uspto-grants-2005_10 |
| ORD ID | ord-7efc57ded6f7404794f1c0a62996d328 |
| 출처 메모 | uspto-grants-2005_10 |