Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methylimidazole → 2-(2-Methyl-1H-imidazol-1-yl)ethan-1-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methylimidazole | HCID 12749 | — |
| 반응물 | 2-Chloroethylamine hydrochloride | HCID 9793737 | — |
| 생성물 | 2-(2-Methyl-1H-imidazol-1-yl)ethan-1-amine | HCID 3157480 | 47% |
반응 단계
2-(2-Methylimidazol-1-yl)ethylamine was prepared from 2-methylimidazole and 2-chloroethylamine hydrochloride using the method described in Step B of Example 1. This material was obtained as a light yellow oil in 47% yield. 1H NMR (300 MHz, CD3OD) δ 6.95 (br s, 1H), 6.82 (br s, 1H), 4.90 (bs, 2H), 3.90 (t, J=6.9 Hz, 2H), 2.93 (t, J=6.9 Hz, 2H), 2.35 (s, 3H); MS (APCI) m/z 126 [M+H]+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07307094B2 |
| 출처 데이터셋 | uspto-grants-2007_12 |
| ORD ID | ord-6b9488b66cbe4438850a1055f7b1eecf |
| 출처 메모 | uspto-grants-2007_12 |