Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl 3-formyl-1H-indole-7-carboxylate → Methyl 3-(hydroxyiminomethyl)indole-7-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl 3-formyl-1H-indole-7-carboxylate | HCID 762965 | — |
| 반응물 | Hydroxyammonium hydrochloride | HCID 22029257 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Methyl 3-(hydroxyiminomethyl)indole-7-carboxylate | HCID 136376389 | 97.4% |
반응 단계
5 g of methyl 3-formylindole-7-carboxylate (0.024 mol) are added to a solution of 0.03 mol of hydroxylammonium hydrochloride in dimethylformamide. The reaction mixture is heated at 125° for one hour and subjected to conventional work-up, giving 5.1 g of methyl 3-(hydroxyiminomethyl)indole-7-carboxylate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07312342B2 |
| 출처 데이터셋 | uspto-grants-2007_12 |
| ORD ID | ord-35682b06232f4d1fb4ecb9fe1e25772f |
| 출처 메모 | uspto-grants-2007_12 |