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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 972021생성일: 2026년 10월 24일

Potassium Hydroxide → Glycerol tris[2-hydroxy-3-(7,7,8,9,9-pentamethyl-2,4-dioxo-1,3,8-triazaspiro[4.5]dec-3-yl)propyl]ether

https://huagongshe.com/ko/reaction/972021

반응식

참여 물질

역할이름HCID투입량
반응물Potassium HydroxideHCID 14797—
반응물TriglycidylglycerolHCID 25795—
반응물7,7,8,9,9-Pentamethyl-1,3,8-triazaspiro[4.5]decane-2,4-dioneHCID 20481853—
용매MethanolHCID 887—
생성물Glycerol tris[2-hydroxy-3-(7,7,8,9,9-pentamethyl-2,4-dioxo-1,3,8-triazaspiro[4.5]dec-3-yl)propyl]etherHCID 131711585—

반응 단계

12.0 g of 7,7,8,9,9-pentamethyl-1,3,8-triazaspiro[4.5]-decane-2,4-dione, 4.1 g of glycerol tris(2,3-epoxypropyl)ether and 1.1 g of potassium hydroxide were reacted in 80 ml of methanol, following substantially the same procedure as in Example 1. The desired Compound No. 177 was obtained in the form of a white powder, having an Rf value of 0.45 on thin-layer chromatography on silica gel using a 4:4:4:1:1 by volume mixture of benzene, ethyl acetate, chloroform, methanol and triethylamine as developing solvent.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04162246
출처 데이터셋uspto-grants-1979_07
ORD IDord-92d226cb0e284e6eb5648e6b1e540e68
출처 메모uspto-grants-1979_07