참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Nitrobenzene | HCID 7416 | — |
| 반응물 | p-Toluidine | HCID 7813 | — |
| 반응물 | Potassium Acetate | HCID 517044 | — |
| 반응물 | Selenium | HCID 6326970 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 1-(4-Methylphenyl)-3-phenylurea | HCID 572170 | — |
반응 단계
Ten milliliters of nitrobenzene, 100 milliliters of tetrahydrofuran, 1.0 gram potassium acetate, 1.0 gram selenium and 21.4 grams of p-toluidine are charged to the autoclave which is then flushed and pressured to 800 psig with carbon monoxide. The temperature is raised to 180° C. for one hour giving 1-p-tolyl-3-phenylurea as product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04052454 |
|---|
| 출처 데이터셋 | uspto-grants-1977_10 |
|---|
| ORD ID | ord-18802182db8c4af2ae36e5ffa8b87fbd |
|---|
| 출처 메모 | uspto-grants-1977_10 |
|---|
