Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Vinylidene chloride → Acrylic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Vinylidene chloride | HCID 6366 | — |
| 반응물 | Methyl Ethyl Ketone | HCID 6569 | — |
| 반응물 | Methyl Acrylate | HCID 7294 | — |
| 생성물 | Acrylic Acid | HCID 6581 | — |
| 생성물 | Allyl chloroacetate | HCID 76206 | — |
반응 단계
Vinylidene chloride (60.5g) was mixed together with 28.8. of methyl acrylate. 10.6 g of acrylic acid and 11.1 g of allyl monochloroacetate in 100 ml of methyl ethyl ketone to give a 50% by volume solution, the temperature of the methyl ethyl ketone being 40° C. Then as copolymerisation initiator 1.0 g of 2, 2'- azobisisobutyronitrile was added to the monomer solution. The solution was maintained at 40° C until the copolymerisation was complete, which took 6 days.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04052528 |
| 출처 데이터셋 | uspto-grants-1977_10 |
| ORD ID | ord-0b7d9ba02a0348b8864b5058b14de80c |
| 출처 메모 | uspto-grants-1977_10 |