Cyclohexyl isocyanate → HCID 178485086, 화합물
반응식
[CH3:1][N:2]([CH3:7])[C:3]([NH2:6])=[N:4][CH3:5].[CH:8]1([N:14]=[C:15]=[O:16])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1>C1(C)C=CC=CC=1>[CH:8]1([NH:14][C:15]([N:6]=[C:3]([NH:4][CH3:5])[N:2]([CH3:7])[CH3:1])=[O:16])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1참가 물질
4
실험 절차
To 60.6 parts by weight of 1,1,2-trimethylguanidine in 600 parts by volume of toluene are added dropwise with cooling 75 parts by weight of cyclohexyl isocyanate. After evaporation of the solvent in vacuo, the product is recrystallized from acetonitrile to yield 2-cyclohexylcarbamoyl-1,1,3-trimethylguanidine, m.p. 121°-124° C.
후처리
- customAfter evaporation of the solvent in vacuo
- customthe product is recrystallized from acetonitrile
출처 및 근거
- ORD 기록
- ord-bd00a2121e2842f294c6457713ad36d7
- 출처 데이터셋
- uspto-grants-1977_10
- 특허 번호
- US04053299
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