Acetic Acid → Molybdate (Mo2O72-), hydrogen, compd. with 1,3,5-triazine-2,4,6-triamine (1:2:1)

HRID 972462

반응식

HRID 972462 반응식
[C:1](O)(=O)C.[N:5]1[C:12]([NH2:13])=[N:11][C:9]([NH2:10])=[N:8][C:6]=1[NH2:7]>[NH4+].[O-][Mo]([O-])(=O)=O.[O-][Mo]([O-])(=O)=O.O>[CH4:1].[C:6]1([NH2:7])[N:8]=[C:9]([NH2:10])[N:11]=[C:12]([NH2:13])[N:5]=1.[C:6]1([NH2:7])[N:8]=[C:9]([NH2:10])[N:11]=[C:12]([NH2:13])[N:5]=1

참가 물질

5

반응물 2

HCID 176Acetic Acid2회HCID 7955Melamine

생성물 1

HCID 103335Molybdate (Mo2O72-), hydrogen, compd. with 1,3,5-triazine-2,4,6-triamine (1:2:1)

시약·촉매·용매 2

HCID 21895884Azanium bis(dioxido(dioxo)molybdenum)촉매HCID 962Water용매3회

실험 절차

Melamine molybdate was prepared in the presence of acetic acid as follows. 10 grams of melamine, 9.52 grams of acetic acid, and 250 ml water were dissolved together by refluxing in a 500 ml round-bottomed flask equipped with a stirrer and water-cooled condenser. 26.95 grams of ammonium dimolybdate was dissolved in 50 ml. hot water and then added to the first solution. A white precipitate formed immediately.

후처리

  1. temperatureby refluxing in a 500 ml round-bottomed flask
  2. customequipped with a stirrer
  3. customA white precipitate formed immediately

출처 및 근거

ORD 기록
ord-f742670e27b647b1bf0c835b60db86de
출처 데이터셋
uspto-grants-1977_10
특허 번호
US04053452

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